Asit Konsantrasyonunun Sol-jel Türevi Y2O3 Yüzey Alanına Etkisi


Gültekin S., Birlik I.

Cukurova 11th International Scientific Researches Conference, Adana, Türkiye, 22 - 24 Ağustos 2023, ss.354, (Özet Bildiri)

  • Yayın Türü: Bildiri / Özet Bildiri
  • Basıldığı Şehir: Adana
  • Basıldığı Ülke: Türkiye
  • Sayfa Sayıları: ss.354
  • Dokuz Eylül Üniversitesi Adresli: Evet

Özet

Yttrium oxide (Y2O3) ceramics have been investigated in detail for many technological

purposes and used as important material in the ceramic industry, ceramic superconductors,

MOS transistors and light-emitting materials. Phosphor materials are important tools for the

efficient utilization of current energy. These materials can be used in various fields such as

display panels, fluorescent paints, and bio-imaging. In this study, Y2O3 phosphor particles with

different surface areas were produced using the sol-gel method. The aim of the study is to

investigate the effect of citric acid concentration used in the solution preparation stage on the

surface area of the final product. Luminescent materials can be more effectively used with

increasing surface area. For this purpose, starting solutions with three different acid

concentrations were prepared. The solutions were prepared to have citric acid concentrations

with respect to the total metal ions (MRCM) at 0.5, 1, and 2 molar concentrations. The organic

contents of the dried solutions were compared using Fourier transform infrared (FTIR)

spectroscopy, and the phase structures of the obtained samples after heat treatment were

analyzed using X-ray diffraction (XRD). The surface areas of the final Y2O3 particles were

measured and characterized using Brunauer-Emmett-Teller (BET) analysis. It is observed that

the acid concentration significantly changed the surface area of Y2O3. The surface areas of the

Y2O3 particles increased with increasing acid concentration. The surface areas of the samples

with MRCM values of 0.5, 1, and 2 were measured as 19.16 m2/g, 32.76 m2/g, and 53.48 m2/g,

respectively. The study showed that the surface area, which affects the luminescent properties

of phosphor materials, can be easily modified using the sol-gel method.