Electrochemical Determination of Sesamol in Foods by Square Wave Voltammetry at a Boron-Doped Diamond Electrode


ASLIŞEN B., KOÇAK Ç. C., KOÇAK S.

ANALYTICAL LETTERS, cilt.53, sa.3, ss.343-354, 2020 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 53 Sayı: 3
  • Basım Tarihi: 2020
  • Doi Numarası: 10.1080/00032719.2019.1650752
  • Dergi Adı: ANALYTICAL LETTERS
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, Aerospace Database, Aquatic Science & Fisheries Abstracts (ASFA), BIOSIS, Biotechnology Research Abstracts, CAB Abstracts, Chimica, Communication Abstracts, Food Science & Technology Abstracts, Metadex, Veterinary Science Database, Civil Engineering Abstracts
  • Sayfa Sayıları: ss.343-354
  • Anahtar Kelimeler: Boron-doped diamond electrode (BDDE), cyclic voltammetry (CV), sesamol, square wave voltammetry (SWV), tahini halva
  • Dokuz Eylül Üniversitesi Adresli: Evet

Özet

Sesamol is a phenolic compound naturally found in sesame seeds. It has beneficial health effects in humans, as it features significant antioxidant activity and has anticancer and anti-aging properties. Therefore, finding a suitable electrode surface for sesamol determination is important. The prominent advantage of boron-doped diamond electrodes is their use in many sensing platforms without the need for the surface modification. This study represents the first time that sesamol has been determined using boron-doped diamond electrodes in acidic media by square wave voltammetry. Linear responses of sesamol were obtained in the concentration range from 0.2 mu M to 1000 mu M, and the detection limit was determined to be 85 nM based on a signal-to-noise ratio of 3. The relative standard deviations were 2.1% for a 1 mu M standard with three measurements.