Synthesis of NiCrAl/MgO-ZrO2 cermet powders by chemical method for functionally graded coatings


Celik E., Birlik I., Karakas Y.

JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, cilt.209, sa.2, ss.695-699, 2009 (SCI-Expanded, Scopus) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 209 Sayı: 2
  • Basım Tarihi: 2009
  • Doi Numarası: 10.1016/j.jmatprotec.2008.02.080
  • Dergi Adı: JOURNAL OF MATERIALS PROCESSING TECHNOLOGY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.695-699
  • Anahtar Kelimeler: NiCrAl/MgO-ZrO2, Cermet, Chemical synthesis, FGM
  • Dokuz Eylül Üniversitesi Adresli: Evet

Özet

Functionally graded materials (FGMs) are receiving great attention as they provide optimum thermal and mechanical properties without a discrete interface between two materials. In order to control the chemical composition and microstructure of FGMs, NiCrAl/MgO-ZrO2 cermet powders were successfully developed in the present work. The NiCrAl/MgO-ZrO2 powders were synthesized from a solution of NiCrAl, ZrO2 and Mg hydroxide carbonate precursors using chemical synthesis. The powders were dried at 125 degrees C for 3 h and then pellet samples were sintered at 1381 degrees C for 30 min under N-2-5%H-2 atmosphere. The powders were characterized by scanning electron microscope, energy dispersive spectroscopy, Xray mapping and X-ray diffraction. The obtained results showed that the optimum particle sizes of NiCrAl/MgO-ZrO2 powders were between 45 and 90 mu m. Microstructural studies have shown a uniform mixing in the cermet powders. it was also found that NiCrAl/MgO-ZrO2, Ni, Cr and Ni5Al3 phases were present in the cermet powder. (c) 2008 Elsevier B.V All rights reserved.